Chemistry


The Chemical analysis of impact sites will help in determining the impacting particulate origin.  Impacts are classified as being caused by either space debris (man-made) or micrometeoroids (natural), or unknown in the case where data was inconclusive (the majority of cases).

The chemical analysis schedule consists of a series of analyses to be performed at the Venture Business Laboratory of the Tokyo Institute of Technology.  A JEOL JSM 5310LV microscope with Energy-Dispersive X-Ray system (EDX) is used which requires no pre-analysis conducting coating to be applied to the sample, thus minimising additional contamination.
 

Round Surfaces
1 PLU1 and PLU4 SSM
2 MLI

The combined results of the chemical analysis will be published in an SFU Chemical Analysis Portfolio. The following tables list the SSM impacts analysed and the results obtained so far. Click on the image to retrieve either an SEM Image of the impact site or the EDX Spectra for that site.
 

PLU-1 SSM
ID Particle Origin SEM Image EDX Spectra
P14  
K12  
T4  
H10  
V13  
Z11  
F2  
M10B  
M10C  
S10  
L9  
W11  
N4  
P11  
U11  
K9  
S14  
Q1  
C5  
X6  
W7  
A5  
W14  
015  
B6  
O10  
U10  
B2  
G12  
V11  
D14  
J1  
Y9  
Q13  
B11  
P10  
N13  
C4  
P5  
L12  
A10  
E7B  
O1  
E7A  
U15A  
I15A  
H6  
K4  
 
PLU-4 SSM
ID Particle Origin SEM Image EDX Spectra
M15B   <
G5   <
J7   <
B12   <
J1B   <
I4   <
R7   <
M8   <
R14   <
J14   <
K9  
V6  
H5  
W13  
X6  
B11A  
N14  
B2  
P2  
M15  
I7  
M12B  
J2  
Q2  
S6  
P8A  
Z1  
L12  
D9  
L2  
X3  
E10  
M12A  
K1  
L3  
V3  
I10  
P8B  
Y13  
R13  
U6  
K10  
N13  
O1  
AB7B  
A9  
AA10  

PLU-2 MLI

The spectra for 56 impacts on the MLI of PLU-2 are included below.  More data will be added as the chemical analysis progresses.

For each impact site, the investigations strategy was as follows:

    1) peel off the top MLI layer and mount it on the special SEM sample holder, face up.
    2) repeat for the last MLI layer, i.e. the one which finally stopped the impactor, mounting it face up also.
    3) discard all intervening layers, as well as those layers not perforated by the target

The reasoning behind this strategy was simply that we presumed that the top and bottom layers would be the ones most likely to have retained impactor residues, particularly the bottom layer, for the impactor would by that stage have slowed down to the extent that complete vaporisation was unlikely (however a large amount of MLI material from the upper layers will probably have been mixed in with the projectile).

Before searching for impactor residues we took a low-magnification image of the impact site (one for the top and bottom layers respectively) and the surrounding area using the SEM, on which we marked the precise areas that we subjected to EDX analysis.  In general it was quite easy to distinguish between contamination, and it was found that a number of sites were severely contaminated during sample preparation.

PLU-2 MLI consisted of seven separate sheets, six of which were found to contain impacts.  Below is a table summarising our findings, below which are links to download files containing the image overviews of the impacts sites with ...... We decided not to provide links to individual impact sites.
 
PLU-2 MLI #1
ID # Particle Origin SEM Images EDX Spectra
1 *
2
3
4
5
6
7
8
9
10 *
11 *
12 *
13 *
14 *
15 *
16 *
17 *
18 *
19 *
20 *
21 *
22 *
23 *
24
25 *
26 *

Download all the PLU-2 MLI No. 1 SEM Images.

Download all the PLU-2 MLI No. 2 SEM Images.

Download all the PLU-2 MLI No. 3 SEM Images.

Download all the PLU-2 MLI No. 5 SEM Images.

Download all the PLU-2 MLI No. 6 SEM Images.

Download all the PLU-2 MLI No. 7 SEM Images.

For further information please contact seed@jaxa.jp .

As data becomes available it will be added to this page

Sorry for the inconvenience
 
 


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